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Transcript
Cristina Sola Larrañaga
Laboratory of Atomic and Molecular Structure.
1. Spin-orbit coupling constant determination for K doublet 2. Ionization deppressor effect. [Na] and [K] quantification in Aquarius
Atomic emission
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Atomic emissionQuantum numbers Spin-orbit interaction Atomic Emission Spectroscopy (AES) Experimental Data
Index
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Fireworks and atomic emission
Atomic emission spectra
Info
Atomic emission
Emission
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Rules
Orbitals
Play
Quantum numbers
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Spin-orbit coupling Example (p1 electrons)
Spin-orbit coupling Energy Equation Derivation
Spin-orbit interaction
Spin-Orbit interaction
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Chemical
Ionization
Spectral
Interferences
Flame Atomic Emission Spectroscopy
Atomic Emission Spectroscopy
Spectroscopy
Atomic Emission Spectroscopy
PC/Software
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Nebuliser
Monochromator
Fotomultiplier
Burner
Flame Atomic Emission Spectroscopy
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Ionization interference study for Na and K. [Na] and [K] quantification in Aquarius
Spin-orbit coupling constan determination for K doublet
Experimental:
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Example for Na
nm
2P1/2
2P3/2
Experimental: Spin-orbit coupling constant determination for K doublet
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
4 Samples: Na: 2ml Aquarius D10 in 100 ml (with or without Li) K: 2 ml Aquarius in 100 ml (with or without Li)
Standard curve calibration with Li
Standard curve calibration without Li
Experimental: Ionization interference study
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Ionization interference study for Na and K. [Na] and [K] quantification in Aquarius
Spin-orbit coupling constan determination for K doublet
Data
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
Data for a 2ppm K solution
Data: Spin-orbit coupling constant determination for K doublet
Laboratory of Atomic and Molecular Structure.
Cristina Sola Larrañaga
4 Samples: Na with Li: 4265 Na without Li: 4010 K with Li: 4224 K without Li: 3926
Data: Ionization interference study